By Antonius Kettrup
This can be the 5th quantity in a world sequence of analytical tools for the choice of toxicants within the air on the place of work. All tools are trustworthy, reproducable and meet the necessities for qc. The research of the degrees of harmful components within the air inhaled by means of employees within the chemical and related operating environments is critical to observe adherence to statutory focus limits and to guard the employees from the antagonistic results of such ingredients.
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Additional resources for Analyses of Hazardous Substances in Air, Volume 5
14 mg/m3 (injection of 5 and 25 µL of a solution with a concentration of 114 µg/mL a,a-dichlorotoluene on the collection phase followed by drawing 20 L of air through the tube). The relative humidity in both cases was max. 65 %. 61 a,a-Dichlorotoluene 2 Sampling with a pump and adsorption on Tenax, gas chromatography after desorption This method permits the determination of a,a-dichlorotoluene concentrations in working areas averaged over the sampling time after personal or stationary sampling.
Analyses of Hazardous Substances in Air,Volume 5. DFG, Deutsche Forschungsgemeinschaft Copyright # 2002 Wiley-VCH Verlag GmbH ISBNs: 3-527-27046-9 (Hardcover); 3-527-60019-1 (Electronic) 27 Bis(chloromethyl)ether Federation of the Employment Accidents Insurance Institutions of Germany (Hauptverband der Berufsgenossenschaften) Centre for Accident Prevention and Occupational Medicine Alte Heerstraße 111, 53757 Sankt Augustin Expert Committee Chemistry Carcinogenic substances Established methods Order number : Issue: BGI 505-6E July 1997 Method for the determination of bis(chloromethyl)ether (BCME) (1,1'-dichlorodimethyl ether) Method tested and recommended by the Berufsgenossenschaften for the determination of BCME in working areas after discontinuous sampling: 1 Sampling with a pump and adsorption on Porapak Q, gas chromatography after desorption.
The adsorption tube is then connected directly on the inlet side to an empty adsorption tube (pre-tube), which is closed with a cap with a borehole 32 Analytical Methods of 2 mm in diameter. The pump is started. With an injection syringe 1 mL of MIBK calibration gas (cf. Sect. 3) is then slowly injected into the pre-tube through the cap ± as far as the injection needle reaches ± within about 15 to 30 seconds. The pump should be allowed to run for at least one minute more. The tubes are then separated and the filled adsorption tube closed again with the caps.